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Engineering
Polimer Bazlı Nanokompozitlerin Dielektrik Özelliklerini Geliştirmek İçin Kaplin Maddesi Uygulaması
Polimer Bazlı Nanokompozitlerin Dielektrik Özelliklerini Geliştirmek İçin Kaplin Maddesi Uygulaması
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JoVE Journal Engineering
Application of a Coupling Agent to Improve the Dielectric Properties of Polymer-Based Nanocomposites

Polimer Bazlı Nanokompozitlerin Dielektrik Özelliklerini Geliştirmek İçin Kaplin Maddesi Uygulaması

Full Text
6,393 Views
06:34 min
September 19, 2020

DOI: 10.3791/60916-v

Haotian Li1,2,3, Dong Zhang4, Zechen Li4, Leyi Li5, Jiachen Liu1, Yugui Li1,2

1Taiyuan University of Science and Technology, 2Heavy Machinery Engineering Research Center of the Ministry of Education, 3Laboratory of Magnetic and Electric Functional Materials and Applications,The Key Laboratory of Shanxi Province, 4Beijing Institute of Aerospace System Engineering, 5Department of Electrical and Information Engineering,Sichuan College of Architectural Technology

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Overview

This study presents a low-cost solution-casting process to enhance the compatibility between polymer matrices and surface modified BaTiO3 fillers. The method effectively improves the energy density of polymer-based nanocomposites.

Key Study Components

Area of Science

  • Polymer Science
  • Nanocomposites
  • Energy Storage Materials

Background

  • Surface modification of ceramic fillers can enhance their compatibility with polymer matrices.
  • Improved wettability at the ceramic-polymer interface is crucial for performance.
  • High-performance film capacitors require flexible composite materials.
  • Commercial coupling agents can be used to modify ceramic nanofillers.

Purpose of Study

  • To develop a method for improving the energy storage performance of polymer-based nanocomposites.
  • To investigate the effects of coupling agents on the properties of ceramic-polymer interfaces.
  • To provide a cost-effective solution for producing flexible composites.

Methods Used

  • Preparation of KH550 solution with ethanol-water solvent.
  • Ultrasonication treatment of BaTiO3 nanoparticles in KH550 solutions.
  • Coating of BT nanoparticles with varying amounts of coupling agent.
  • Evaporation of solvent at controlled temperatures in a vacuum oven.

Main Results

  • Good wettability was achieved at the ceramic-polymer interface.
  • Enhanced energy storage performances were observed with optimal coupling agent amounts.
  • The method is suitable for the preparation of flexible composites.
  • Results indicate potential applications in high-performance film capacitors.

Conclusions

  • The developed solution-casting process is effective and low-cost.
  • Surface modification significantly improves composite performance.
  • This approach can facilitate advancements in energy storage technologies.

Frequently Asked Questions

What is the main focus of this study?
The study focuses on enhancing the compatibility of polymer-based nanocomposites using surface modified BaTiO3 fillers.
How does surface modification affect energy storage?
Surface modification improves wettability and enhances the energy storage performance of the composites.
What method was used for the surface modification?
A commercial coupling agent was used to modify the surface of the ceramic nanofillers.
What are the potential applications of this research?
The research has potential applications in the production of high-performance film capacitors.
Is the method described cost-effective?
Yes, the solution-casting process is described as simple and low-cost.

Burada, kompozitlerin enerji yoğunluğunu etkili bir şekilde artırabilen yüzey modifiye edilmiş BaTiO3 dolgu maddeleri kullanarak dolgu ve polimer bazlı nanokompozitlerin matrisi arasındaki uyumluluğu artırmak için basit ve düşük maliyetli bir çözüm döküm işlemi gösteriyoruz.

Ticari bağlantı ajanının kullanılmasının seramik nanofillerin yüzeyini değiştirebileceği, bu nedenle seramik-polimer arabiriminde iyi ıslaklık sağlandığı ve uygun miktarda bağlantı ajanı ile gelişmiş enerji depolama performansları elde edildiği kanıtlanmıştır. Bu çalışma ile geliştirilen yöntem, yüksek performanslı film kapasitörleri üretimi için son derece arzu edilen esnek kompozitlerin hazırlanmasında kullanılabilir. KH550 çözeltisini 15 dakika ultra-sonication tarafından yüzde 95 ağırlık yüzde etanol su çözücü ile hazırlayın.

KH550 çözümlerindeki BT nano partiküllerini 30 dakika ultra-sonication ile tedavi edin. Bu işlemde, beş mililitre lik bir hacimle KH550 seyreltik çözeltisindeki bağlantı maddesinin bir, iki, üç, dört ve beş ağırlıkile kaplanmış KH550 ve BT nano partiküllerinin ağırlıklarını ölçün. 80 derece C'deki su-etanol çözücüsi 5 saat, sonra 120 derece C'ye kadar vakumlu fırında 12 saat buharlaştırın.

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