Name: Kaskad Tasarım Oksidasyonu ve Yüksek Bazik İndirgeme Reaksiyonları Kullanılarak Grafen Oksit ve İndirgenmiş Grafen Oksitin Ölçeklenebilir Sentezleri (Video) | JoVE Journal
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Description: Öğrenin, kaskad tasarım oksidasyonu ve yüksek bazik indirgeme reaksiyonları kullanarak grafen oksit ve indirgenmiş grafen oksitin ölçeklenebilir sentez yöntemlerini. Bu protokoller nanomalzeme üretiminde güvenliği ve verimliliği artırır.

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<li>Lakhe, P., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Graphene+oxide+synthesis%3A+reaction+calorimetry+and+safety%5BTitle%5D)+AND+%22Ind+Eng+Chem+Res%22%5BJournal%5D)">Graphene oxide synthesis: reaction calorimetry and safety.</a> Ind Eng Chem Res. 59 (19), 9004-9014 (2020).</li>
<li>Lee, S., Oh, J., Ruoff, R. S., Park, S. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Residual+acetone+produces+explosives+during+the+production+of+graphite+oxide%5BTitle%5D)+AND+%22Carbon%22%5BJournal%5D)">Residual acetone produces explosives during the production of graphite oxide.</a> Carbon. 50 (3), 1442-1444 (2012).</li>
<li>Kummer, A., Varga, T. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((What+do+we+know+already+about+reactor+runaway%3F+-+A+review%5BTitle%5D)+AND+%22Process+Saf+Environ+Prot%22%5BJournal%5D)">What do we know already about reactor runaway? - A review.</a> Process Saf Environ Prot. 147, 460-476 (2021).</li>
<li>Li, D., Muller, M. B., Gilje, S., Kaner, R. B., Wallace, G. G. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Processable+aqueous+dispersions+of+graphene+nanosheets%5BTitle%5D)+AND+%22Nat+Nanotechnol%22%5BJournal%5D)">Processable aqueous dispersions of graphene nanosheets.</a> Nat Nanotechnol. 3, 101(2008).</li>
<li>Yang, X., Zhu, J., Qiu, L., Li, D. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Bioinspired+effective+prevention+of+restacking+in+multilayered+graphene+films%3A+towards+the+next+generation+of+high-performance+supercapacitors%5BTitle%5D)+AND+%22Adv+Mater%22%5BJournal%5D)">Bioinspired effective prevention of restacking in multilayered graphene films: towards the next generation of high-performance supercapacitors.</a> Adv Mater. 23, 2833-2838 (2011).</li>
<li>Tarcan, R., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Reduced+graphene+oxide+today%5BTitle%5D)+AND+%22J+Mater+Chem+C%22%5BJournal%5D)">Reduced graphene oxide today.</a> J Mater Chem C. 8, 1198(2020).</li>
<li>Agarwal, V., Zetterlund, P. B. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Strategies+for+reduction+of+graphene+oxide+-+A+comprehensive+review%5BTitle%5D)+AND+%22Chem+Eng+J%22%5BJournal%5D)">Strategies for reduction of graphene oxide - A comprehensive review.</a> Chem Eng J. 405, 127018(2021).</li>
<li>Luo, J., Kim, J., Huang, J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Material+processing+of+chemically+modified+graphene%3A+some+challenges+and+solutions%5BTitle%5D)+AND+%22Acc+Chem+Res%22%5BJournal%5D)">Material processing of chemically modified graphene: some challenges and solutions.</a> Acc Chem Res. 46 (10), 2225-2234 (2013).</li>
<li>Fan, X., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Deoxygenation+of+exfoliated+graphite+oxide+under+alkaline+conditions%3A+a+green+route+to+graphene+preparation%5BTitle%5D)+AND+%22Adv+Mater%22%5BJournal%5D)">Deoxygenation of exfoliated graphite oxide under alkaline conditions: a green route to graphene preparation.</a> Adv Mater. 20 (23), 4490-4493 (2008).</li>
<li>Paredes, J. I., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Environmentally+friendly+approaches+toward+the+mass+production+of+processable+graphene+from+graphite+oxide%5BTitle%5D)+AND+%22J+Mater+Chem%22%5BJournal%5D)">Environmentally friendly approaches toward the mass production of processable graphene from graphite oxide.</a> J Mater Chem. 21 (2), 298-306 (2011).</li>
<li>Le, N. H., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Solution-processable+conductive+micro-hydrogels+of+nanoparticle%2Fgraphene+platelets+produced+by+reversible+self-assembly+and+aqueous+exfoliation%5BTitle%5D)+AND+%22J+Mater+Chem+A%22%5BJournal%5D)">Solution-processable conductive micro-hydrogels of nanoparticle/graphene platelets produced by reversible self-assembly and aqueous exfoliation.</a> J Mater Chem A. 1, 12900(2013).</li>
<li>Le, H. N., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Sonochemical+synthesis+of+bioinspired+graphene+oxide-zinc+oxide+hydrogel+for+antibacterial+painting+on+biodegradable+polylactide+film%5BTitle%5D)+AND+%22Nanotechnology%22%5BJournal%5D)">Sonochemical synthesis of bioinspired graphene oxide-zinc oxide hydrogel for antibacterial painting on biodegradable polylactide film.</a> Nanotechnology. 35, 305601(2024).</li>
<li>Le, H. N., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Melt+processing+of+graphene-coated+polylactide+granules+for+producing+biodegradable+nanocomposite+with+higher+mechanical+strength%5BTitle%5D)+AND+%22Polym+Plast+Technol+Mater%22%5BJournal%5D)">Melt processing of graphene-coated polylactide granules for producing biodegradable nanocomposite with higher mechanical strength.</a> Polym Plast Technol Mater. 63 (11), 1421-1437 (2024).</li>
<li>Le, H. N., Nguyen, L. N. L., Dao, T. B. T., Nguyen, T. D., Ha Thuc, C. N. Highly tough and antibacterial nanocomposite film of poly(vinyl alcohol)/graphene-oxide-ZnO for biomedical application. <a target="_blank" href="http://scholar.google.com/scholar?hl=en&safe=off&q=author%3aLe%2C+HN+%22Int+J+Nanotechnol%22">Int J Nanotechnol</a>. (2025), In Press (2025).</li>
<li>Bhujel, R., Rai, S., Deka, U., Swain, B. P. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Electrochemical%2C+bonding+network+and+electrical+properties+of+reduced+graphene+oxide-Fe2O3+nanocomposite+for+supercapacitor+electrodes+applications%5BTitle%5D)+AND+%22J+Alloys+Compd%22%5BJournal%5D)">Electrochemical, bonding network and electrical properties of reduced graphene oxide-Fe2O3 nanocomposite for supercapacitor electrodes applications.</a> J Alloys Compd. 792, 250-259 (2019).</li>
<li>Rai, S., Bhujel, R., Biswas, J., Swain, B. P. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Effect+of+electrolyte+on+the+supercapacitive+behaviour+of+copper+oxide%2Freduced+graphene+oxide+nanocomposite%5BTitle%5D)+AND+%22Ceram+Int%22%5BJournal%5D)">Effect of electrolyte on the supercapacitive behaviour of copper oxide/reduced graphene oxide nanocomposite.</a> Ceram Int. 45 (11), 14136-14145 (2019).</li>
<li>Rai, S., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Synthesis%2C+characterizations%2C+and+electrochemical+studies+of+ZnO%2Freduced+graphene+oxide+nanohybrids+for+supercapacitor+application%5BTitle%5D)+AND+%22Mater+Today+Chem%22%5BJournal%5D)">Synthesis, characterizations, and electrochemical studies of ZnO/reduced graphene oxide nanohybrids for supercapacitor application.</a> Mater Today Chem. 20, 100472(2021).</li>
<li>Singh, W. I., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Fabrication+and+Characterization+of+Reduced+GrapheneOxide%2FPolyaniline%2FPoly%28Caprolactone%29+Electrospun+Nanofiber%5BTitle%5D)+AND+%22Arab+J+Sci+Eng%22%5BJournal%5D)">Fabrication and Characterization of Reduced GrapheneOxide/Polyaniline/Poly(Caprolactone) Electrospun Nanofiber.</a> Arab J Sci Eng. 47, 925-934 (2022).</li>
<li>Chaltash, F., Chekin, F., Vahdat, S. M. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Magnetite+Reduced+Graphene+Oxide%2FOrdered+Mesoporous+Carbon+Nanocomposite+as+Effective+Adsorbent+for+Removal+of+2-Naphthol+in+Wastewater%5BTitle%5D)+AND+%22Curr+Anal+Chem%22%5BJournal%5D)">Magnetite Reduced Graphene Oxide/Ordered Mesoporous Carbon Nanocomposite as Effective Adsorbent for Removal of 2-Naphthol in Wastewater.</a> Curr Anal Chem. 20 (6), 410-417 (2024).</li>
<li>Behrouzifar, F., Shahidi, S. A., Chekin, F., Hosseini, S., Ghorbani-HasanSaraei, A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Colorimetric+assay+based+on+horseradish+peroxidase%2Freduced+graphene+oxide+hybrid+for+sensitive+detection+of+hydrogen+peroxide+in+beverages%5BTitle%5D)+AND+%22Spectrochim+Acta+A+Mol+Biomol+Spectrosc%22%5BJournal%5D)">Colorimetric assay based on horseradish peroxidase/reduced graphene oxide hybrid for sensitive detection of hydrogen peroxide in beverages.</a> Spectrochim Acta A Mol Biomol Spectrosc. 257, 119761(2021).</li>
<li>Seyedi, S. H., Shahidi, S. A., Chekin, F., Ghorbani-HasanSaraei, F. A., Limooei, M. B. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Simultaneous+Determination+of+1-Naphthol+and+2-Naphthol+in+Waters+by+Electrochemical+Sensor+Based+on+Magnetite+Porous+Reduced+Graphene+Oxide%2FCarbon+Nanotube+Hybrid%5BTitle%5D)+AND+%22Russ+J+Electrochem%22%5BJournal%5D)">Simultaneous Determination of 1-Naphthol and 2-Naphthol in Waters by Electrochemical Sensor Based on Magnetite Porous Reduced Graphene Oxide/Carbon Nanotube Hybrid.</a> Russ J Electrochem. 59, 1138-1150 (2023).</li>
<li>Vatandost, E., Ghorbani-HasanSaraei, A., Chekin, F., Raeisi, S. N., Shahidi, S. A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Green+tea+extract+assisted+green+synthesis+of+reduced+graphene+oxide%3A+Application+for+highly+sensitive+electrochemical+detection+of+sunset+yellow+in+food+products%5BTitle%5D)+AND+%22Food+Chem+X%22%5BJournal%5D)">Green tea extract assisted green synthesis of reduced graphene oxide: Application for highly sensitive electrochemical detection of sunset yellow in food products.</a> Food Chem X. 6, 100085(2020).</li>
<li>Naderi, N., Sabeti, B., Chekin, F. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Fe3O4+nanoparticles+decorated+reduced+graphene+oxide+and+carbon+nanotubes-based+composite+for+sensitive+detection+of+imatinib+in+plasma+and+urine%5BTitle%5D)+AND+%22J+Electrochem+Sci+Eng%22%5BJournal%5D)">Fe3O4 nanoparticles decorated reduced graphene oxide and carbon nanotubes-based composite for sensitive detection of imatinib in plasma and urine.</a> J Electrochem Sci Eng. 14 (2), 119-133 (2024).</li>
<li>Amiri, M., Hashemi, Z., Chekin, F. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Zinc+oxide+nanoparticles+decorated+nitrogen+doped+porous+reduced+graphene+oxide-based+hybrid+to+sensitive+detection+of+hydroxychloroquine+in+plasma+and+urine%5BTitle%5D)+AND+%22J+Mater+Sci%3A+Mater+Med%22%5BJournal%5D)">Zinc oxide nanoparticles decorated nitrogen doped porous reduced graphene oxide-based hybrid to sensitive detection of hydroxychloroquine in plasma and urine.</a> J Mater Sci: Mater Med. 36, 4(2025).</li>
</ol>

<table><tbody><tr><td>Amonyak çözeltisi %25 - %28</td><td>Xilong Bilimsel Şirketi</td><td>1336-21-6</td><td></td></tr><tr><td>Grafit tozu</td><td>Şanghay Zhanyun Kimya Şirketi</td><td>7782-42-5</td><td></td></tr><tr><td>Hidroklorik asit %36</td><td>Xilong Bilimsel Şirketi</td><td>7647-01-0</td><td></td></tr><tr><td>Hidrojen peroksit çözeltisi %30</td><td>Xilong Bilimsel Şirketi</td><td>7722-84-1</td><td></td></tr><tr><td>Potasyum permanganat %99,5</td><td>Duc Giang Kimyasallar Grubu</td><td>7722-64-7</td><td></td></tr><tr><td>Sülfürik asit %97</td><td>Xilong Kimya Şirketi</td><td>7664-93-9</td><td></td></tr></tbody></table>

kaskad tasarım oksidasyonu ve yüksek bazik İndirgeme reaksiyonları kullanılarak grafen oksit ve İndirgenmiş grafen oksitin Ölçeklenebilir sentezleri

Scalable Syntheses of Graphene Oxide and Reduced Graphene Oxide using Cascade Design Oxidation and Highly Basic Reduction Reactions

Kaskad tasarımı, oksidasyon reaksiyonu ve yüksek bazik indirgeme reaksiyonunun deneysel şemaları Şekil 1'de sunulmuştur. Daha önce açıklandığı gibi, grafit oksidasyon reaksiyonu iki ana kademeli adımiçerir 3,8. Protokolde, 1.1 ve 1.2 adımlarından sonra 1.3 adımına ulaşılmıştır (Şekil 1A). Karışım sıcaklığının oda sıcaklığından yaklaşık 48-52 °C'ye yükselmesi, grafit ve Mn(VII) bileşiği arasında ekzotermi...

Kaskad Tasarım Oksidasyonu ve Yüksek Bazik İndirgeme Reaksiyonları Kullanılarak Grafen Oksit ve İndirgenmiş Grafen Oksitin Ölçeklenebilir Sentezleri

This present work describes the scalable synthetic methods of oxidation and reduction reactions for producing graphene oxide and reduced graphene oxide ...

scalable-syntheses-graphene-oxide-reduced-graphene-oxide-using

Research

JoVE Journal

Chemistry

Kimya

Görünür bir ışık ve plasmonik nanoparçacık kullanılarak düşük grafin oksit hazırlanması için bir basit bir protokol tarif edilmektedir.

Plasmonik Nanoparçacık Kullanma Grafen Oksit Görünür ışık Bağlı Azaltma

Bu video yöntemi, polimer öncülerinden türetilen yüksek yüzey alanlı, monolitik 3D grafen bazlı malzemelerin yanı sıra tek katmanlı grafen oksitin sentezini açıklar.

Sentezi ve 3D Nano-grafen Malzemelerin fonksiyonalizasyonu: Grafen Aerogels ve Graphene Makro Meclisleri

nanosheets katmanlı malzeme, sıvı pul pul dökülme için bir protokol, mikroskopik ve spektroskopik tekniklerle boyutu seçimi ve boyut ölçümü sunulmuştur.

Sıvı dağılmış Geçiş Metal dikalkogenid Kontrollü Boyutu Nanosheets ve Kalınlığının Hazırlanması: Sanat Protokolü Bir Devlet

Burada, biz sentezi için bir iletişim kuralı mevcut ve elektrokimyasal test geçiş metalleri tek atomlarının grafen boş seçici karbon dioksit azaltılması için sulu çözümler karbon monoksit için etkin merkezleri olarak koordine.

Sentez ve elektrokimyasal CO2 azaltılması için geçiş metalleri tek Atom katalizör performans karakterizasyonu

Burada, 3D grafen tabanlı polyhedrons origami gibi kendi kendine yolu ile katlama imalat için bir iletişim kuralı mevcut.

Üç boyutlu grafen tabanlı Polyhedrons Origami gibi kendi kendine yolu ile katlama imalat

Asil-metal tabanlı nanokompozitlerin sürekli ve ölçeklenebilir sentezi için bir roman Fotokatalitik reaktör geliştirilen ve yapısı, çalışma ilkeleri ve ürün kalitesi optimizasyon stratejileri açıklanmıştır.

Metalik nano tanecikleri tam kontrollü birikimi için sürekli akış Fotokatalitik reaktör

Kontrol edilebilir pul boyutu dağıtımları ile grafen nanofluidlerin sentezleme yöntemi sunulmuştur.

Kontrol edilebilir Flake boyutu dağılımları ile Graphene Nanofluids sentezi

Düşük dereceli ısı bol, ama verimli kurtarma hala büyük bir sorundur. Elektrolit olarak KCl ile bir anot olarak katot ve polyanilin olarak grafen oksit kullanarak bir asimetrik termoelektrokimyasal hücre rapor. Bu hücre, düşük sıcaklıklı bölgelerde yüksek ısı-elektrik dönüşüm verimliliği sergileyen, isotermal ısıtma altında çalışır.

Isothermal Operasyon Altında Düşük Dereceli Isı Hasat Için Asimetrik Termoelektrokimyasal Hücre

Çözelti ve yüzey destekli sentezin bir kombinasyonu, nanoyapıların atomik olarak hassas sentezinde yeni yönler açar. Temassız atomik kuvvet mikroskobu (nc-AFM) ile desteklenen taramalı tünelleme mikroskobu (STM), yeni tasarlanan ve üretilen karbon bazlı nano nesnelerin ayrıntılı karakterizasyonunu sağlar.

Çözelti ve Yüzey Kimyası Kombinasyonu ile Sentezlenen Gözenekli Nanografenlerin Mikroskobik Görüntülenmesi

Bu makale, yüksek düzeyde ayarlanabilir, özel yapım bir transfer kurulumuna dayalı olarak modifiye edilmiş bir kuru transfer tekniği kullanan, hassas büküm açılarına sahip yüksek kaliteli grafen bazlı hareli süper kafes cihazları üretmek için optimize edilmiş, deneyime dayalı bir protokol sunmaktadır.

Yüksek Kaliteli Grafen Bazlı Moiré Superlattice Cihazları için Optimize Edilmiş Üretim Prosedürü

Öğrenin, kaskad tasarım oksidasyonu ve yüksek bazik indirgeme reaksiyonları kullanarak grafen oksit ve indirgenmiş grafen oksitin ölçeklenebilir sentez yöntemlerini. Bu protokoller nanomalzeme üretiminde güvenliği ve verimliliği artırır.

Kaskad Tasarım Oksidasyonu ve Yüksek Bazik İndirgeme Reaksiyonları Kullanılarak Grafen Oksit ve İndirgenmiş Grafen Oksitin Ölçeklenebilir Sentezleri (Video) | JoVE Journal

Kaskad Tasarım Oksidasyonu ve Yüksek Bazik İndirgeme Reaksiyonları Kullanılarak Grafen Oksit ve İndirgenmiş Grafen Oksitin Ölçeklenebilir Sentezleri

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