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Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles
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JoVE Journal Chemistry
Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles

Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles

DOI:
10.3791/57667-v

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11:54 min

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June 25, 2018

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, , , , , , ,
1Department of Chemical Engineering,Virginia Polytechnic Institute and State University, 2Center for Integrated Nanotechnologies,Los Alamos National Laboratory, 3Advanced Photon Source,Argonne National Laboratory, 4X-ray Science Division,Argonne National Laboratory, 5Environmental Molecular Science Laboratory,Pacific Northwest National Laboratory

Chapters

  • 00:04Title
  • 00:44Palladium(II) Acetate Recrystallization
  • 03:54Colloidal Pd Nanoparticle Synthesis in Pyridine
  • 06:25Pd Nanoparticle Characterization by Ex Situ Small-Angle X-Ray Scattering (SAXS)
  • 09:52Results: Kinetics of Nucleation and Growth of Pd Nanoparticles in Toluene and Pyridine
  • 11:20Conclusion

Summary

Automatic Translation

Automatic Translation

The main goal of this work is to elucidate the role of capping agents in regulating the size of palladium nanoparticles by combining in situ small angle x-ray scattering (SAXS) and ligand-based kinetic modeling.

Tags

Keywords: PalladiumNanoparticlesNucleationGrowthSAXSKinetic RatesCapping LigandsColloidalMetal OxidesPalladium AcetateVacuum FiltrationCrystallization

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