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Engineering
Preparation of Graphene Liquid Cells for the Observation of Lithium-ion Battery Material
Preparation of Graphene Liquid Cells for the Observation of Lithium-ion Battery Material
JoVE Journal
Engineering
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JoVE Journal Engineering
Preparation of Graphene Liquid Cells for the Observation of Lithium-ion Battery Material

Preparation of Graphene Liquid Cells for the Observation of Lithium-ion Battery Material

Full Text
9,687 Views
10:53 min
February 5, 2019

DOI: 10.3791/58676-v

Joon Ha Chang*1, Jun Young Cheong*1, Hyeon Kook Seo1, Il-Doo Kim1, Jong Min Yuk1

1Department of Materials Science and Engineering,Korea Advanced Institute of Science and Technology

Here, we present a protocol for the fabrication and preparation of a graphene liquid cell for in situ transmission electron microscopy observation, along with a synthesis of electrode materials and electrochemical battery cell tests.

This graphene liquid cell enables transmission electron microscopy for these dynamics in a liquid electrolyte. Such dynamics can provide rich information of the working mechanisms of Lithium-ion batteries and contributes to designing advanced battery devices. The advantages of graphene liquid cell is that it allows TEM imaging in liquid electrolyte providing good spatial resolution and high imaging contrast.

In addition to a superior quality of the image, it can also provide information of various morphological phase and interfacial transitions. With only a written protocol, it is difficult to follow this method because many technical steps are conducted by hand. A lot of the skills require accuracy and precision, where the use of patience is highly recommended.

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