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Characterizing Lewis Pairs Using Titration Coupled with In Situ Infrared Spectroscopy
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Characterizing Lewis Pairs Using Titration Coupled with In Situ Infrared Spectroscopy

Article DOI: 10.3791/60745-v • 07:49 min • February 20th, 2020
February 20th, 2020 •
1, 1
1Department of Chemistry & Biochemistry, Loyola University Chicago

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Here, we present a method for the observation of solution interactions between Lewis acids and bases by employing in situ infrared spectroscopy as a detector for titration under synthetically relevant conditions. By examining solution interactions, this method represents a complement to X-ray crystallography, and provides an alternative to NMR spectroscopy.

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Lewis Pairs Titration In Situ Infrared Spectroscopy Solution Interactions Lewis Acids Carbonyls Mechanistic Insight Carbonyl-centered Reactions Lewis Acid Carbonyl Complexes Real-time Observation Substrates Products Catalyst Fundamental Interactions High-yielding Procedures Equilibrium Change Infrared Spectrum Data Acquisition Software Background Collection Experiment Creation Flame-dried Flask Iron Trichloride Glove Box Inert Atmosphere
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