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Analysis of Volatile and Oxidation Sensitive Compounds Using a Cold Inlet System and Electron Impact Mass Spectrometry
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JoVE 杂志 化学
Analysis of Volatile and Oxidation Sensitive Compounds Using a Cold Inlet System and Electron Impact Mass Spectrometry

Analysis of Volatile and Oxidation Sensitive Compounds Using a Cold Inlet System and Electron Impact Mass Spectrometry

DOI:
10.3791/51858-v

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05:48 min

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September 05, 2014

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1Department of Chemistry, Institute of Organic Chemistry,Bielefeld University

Chapters

  • 00:05Title
  • 01:32Sample Preparation
  • 02:19Measurement of Mass Spectra
  • 03:48After the Measurement
  • 04:43Results: Electron Impact Ionisation Mass Spectra of Volatile and Oxidation Sensitive Compounds
  • 05:25Conclusion

Summary

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This video presents a protocol for the mass spectrometrical analysis of volatile and oxidation sensitive compounds using electron impact ionization. The presented technique is especially of interest for inorganic chemists, working with metal organyls, silanes, or phosphanes which have to be handled using inert conditions, such as the Schlenk technique.

Tags

Volatile CompoundsOxidation Sensitive CompoundsCold Inlet SystemElectron Impact Mass SpectrometrySector Field Mass SpectrometerAir-free ConditionsVacuum ConditionsMetal OrganylsSilanesPhosphanesSchlenk TechniqueInorganic Chemistry

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