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Isolere gratis Carbenes, blandet Dimers og organisk radikaler

Article DOI: 10.3791/59389-v • 10:44 min • April 19th, 2019
April 19th, 2019 •
1, 1, 1
1Department of Chemistry and Pharmacy, Friedrich-Alexander-Universität Erlangen-Nürnberg

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Vi presenterer protokoller for isolering av stabile hetrosyklisk carbenes. Syntese av en syklisk (alkyl)(amino) carbene (CAAC) og en N-hetrosyklisk carbene (NHC) er demonstrert ved hjelp av filteret cannulas og Schlenk teknikk. Vi presenterer videre syntese av den relaterte oksygen-sensitive, rikt blandet "Wanzlick dimer" og den mindre stabile organisk radikale.

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Kjemi problemet 146 kjemi carbenes N-hetrosyklisk carbene NHC syklisk (alkyl)(amino) carbene CAAC filter kanyle Schlenk teknikk air sensitive Wanzlicks likevekt organisk radikale rikt olefins
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