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Photogeneration von N-heterozyklische Carbene: Anwendung bei photoinduzierte ringöffnende Metathese-Polymerisation

Article DOI: 10.3791/58539-v • 12:19 min • November 29th, 2018
November 29th, 2018 •
1, 1, 1, 2,3, 2,3, 2,3, 4, 4
1ICGM, Université de Montpellier, CNRS, ENSCM, 2Institut de Science des Matériaux de Mulhouse (IS2M UMR 7361 CNRS), Université de Haute-Alsace, 3Université de Strasbourg, 4Laboratoire de Chimie des Polymères Organiques (LCPO UMR 5629 ENSCBP), Université de Bordeaux

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Wir beschreiben ein Protokoll zum Photogenerate N-heterozyklische Carbene (NHC) durch UV-Bestrahlung eines 2-Isopropylthioxanthon/Imidazolium Tetraphenylborate-Salz-Systems. Methoden zur Charakterisierung der Photoreleased NHC und erhellen die photochemischen Mechanismus werden vorgeschlagen. Die Protokolle für ringöffnende Metathese Photopolymerisation in Lösung und Miniemulsion veranschaulichen das Potenzial dieses 2-Komponenten-NHC-Photogenerating-Systems.

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Chemie Ausgabe 141 Polymer Ringöffnung Metathese toben Carben NHC Photochemie Miniemulsion Photolyse Photoreactor Photoreactivity
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