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Preparation of a Corannulene-functionalized Hexahelicene by Copper(I)-catalyzed Alkyne-azide Cycloaddition of Nonplanar Polyaromatic Units

Article DOI: 10.3791/53954-v • 09:35 min • September 18th, 2016
September 18th, 2016 •
1, 1, 1
1GIR MIOMeT, IU CINQUIMA, Área de Química Inorgánica, Universidad de Valladolid

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Here, we present a protocol to synthesize a complex organic compound comprised of three nonplanar polyaromatic units, assembled easily with reasonable yields.

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Corannulene-functionalized Hexahelicene Copper(I)-catalyzed Alkyne-azide Cycloaddition Nonplanar Polyaromatic Units Click Chemistry Synthesis Protocol Organic Procedures Free Radical Reactions Carbon-carbon Coupling Host-guest Recognition Debromination 2,15-dimethylhexyl Helicene N-bromosuccinimide Benzoyl Peroxide Carbon Tetrachloride
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