Rivista
/
Chimica
/
Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles
JoVE Journal
Chimica
È necessario avere un abbonamento a JoVE per visualizzare questo.  Accedi o inizia la tua prova gratuita.
JoVE Journal Chimica
Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles

Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles

DOI:
10.3791/57667-v

•

11:54 min

•

June 25, 2018

•

, , , , , , ,
1Department of Chemical Engineering,Virginia Polytechnic Institute and State University, 2Center for Integrated Nanotechnologies,Los Alamos National Laboratory, 3Advanced Photon Source,Argonne National Laboratory, 4X-ray Science Division,Argonne National Laboratory, 5Environmental Molecular Science Laboratory,Pacific Northwest National Laboratory

Capitoli

  • 00:04Titolo
  • 00:44Palladium(II) Acetate Recrystallization
  • 03:54Colloidal Pd Nanoparticle Synthesis in Pyridine
  • 06:25Pd Nanoparticle Characterization by Ex Situ Small-Angle X-Ray Scattering (SAXS)
  • 09:52Results: Kinetics of Nucleation and Growth of Pd Nanoparticles in Toluene and Pyridine
  • 11:20Conclusion

Summary

Traduzione automatica

Traduzione automatica

The main goal of this work is to elucidate the role of capping agents in regulating the size of palladium nanoparticles by combining in situ small angle x-ray scattering (SAXS) and ligand-based kinetic modeling.

Tags

PalladiumNanoparticlesNucleationGrowthSAXSKinetic RatesCapping LigandsColloidalMetal OxidesPalladium AcetateVacuum FiltrationCrystallization

Article

Embed

AGGIUNGI ALLA PLAYLIST

Usage Statistics

Video correlati

Synthesis and Characterization of Functionalized Metal-organic Frameworks

Using Polystyrene-block-poly(acrylic acid)-coated Metal Nanoparticles as Monomers for Their Homo- and Co-polymerization

Reverse Microemulsion-mediated Synthesis of Monometallic and Bimetallic Early Transition Metal Carbide and Nitride Nanoparticles

Generation of Zerovalent Metal Core Nanoparticles Using n-(2-aminoethyl)-3-aminosilanetriol

Photochemical Oxidative Growth of Iridium Oxide Nanoparticles on CdSe@CdS Nanorods

In Situ Detection and Single Cell Quantification of Metal Oxide Nanoparticles Using Nuclear Microprobe Analysis

Molten-Salt Synthesis of Complex Metal Oxide Nanoparticles

Synthesis and Characterization of Amphiphilic Gold Nanoparticles

Synthesis Method for Cellulose Nanofiber Biotemplated Palladium Composite Aerogels

Ion Mobility-Mass Spectrometry Techniques for Determining the Structure and Mechanisms of Metal Ion Recognition and Redox Activity of Metal Binding Oligopeptides

Read Article