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Chemistry

Struktur och samordning Fastställande av peptid-metallkomplex Använda 1D och 2D Published: December 16, 2013 doi: 10.3791/50747
Automatic Translation
1, 1, 2
1Department of Chemistry, The Hebrew University of Jerusalem, 2Wolfson Centre for Applied Structural Biology, The Hebrew University of Jerusalem

Materials

Name Company Catalog Number Comments
Avance DMX 600 MHz Spectrometer Bruker
NMR sample tubes  Wilmad 535-PP
Glove box MBraun LM05-019
Lyophilizer   VirTis benchtopK
Peptide BioChemia Custom made >95% purity
Copper (1) chloride Aldrich 224332
Hydrochloric acid BioLab 231-595-7
Sodium hydroxide Gadot 1310-73-2
d6-Dimethylsulfoxide Aldrich 236926
Deuterium oxide Aldrich 151882

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References

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Struktur och samordning Fastställande av peptid-metallkomplex Använda 1D och 2D<sup&gt; 1</sup&gt; H-NMR
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Shoshan, M. S., Tshuva, E. Y.,… More

Shoshan, M. S., Tshuva, E. Y., Shalev, D. E. Structure and Coordination Determination of Peptide-metal Complexes Using 1D and 2D 1H NMR. J. Vis. Exp. (82), e50747, doi:10.3791/50747 (2013).

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