Turbidity and Total Solids in Surface Water

1. Measuring Turbidity

1. Pour mixed sample water into one turbidity column and fill to the 50-mL line with the sample water.
2. Fill the second “Blank” Turbidity Column with deionized water to the 50-mL line.
3. Place the two tubes side by side and note the difference in clarity. If the black dot is equally clear in both tubes, the turbidity is zero. If the black dot in the sample tube is less clear, proceed to next step.
4. Shake the Standard Turbidity Reagent.
5. Add 0.5 mL of the reagent to the distilled water tube. Use the stirring rod to stir contents.
6. Check for amount of turbidity by looking down through the solution at the black dot. If the turbidity of the sample water is greater than that of the distilled water, continue to add Standard Turbidity Reagent in 0.5-mL increments to the distilled water tube, recording the amount of reagent used and mixing after each addition until the turbidity equals that of the sample.
7. Record the total amount of Turbidity Reagent added.

2. Measuring Total Solids

1. With gloved hands, label a beaker with a grease pencil. Do not use labeling tape because these beakers are going into the oven.
2. Turn on balance and tare it.
3. Place the beaker on the balance and record the weight. Make sure to use a balance that records to the thousandths of a gram. Use gloves to avoid touching the beaker with bare hands and transferring body moisture, thereby changing the weight of the beaker.
4. Using a graduated cylinder, measure 100 mL of the water sample. If the sample has been sitting, swirl the sample water before measuring out the 100 mL.
5. Pour this amount into the beaker.
6. Place the beaker in an oven at 100 °C for 48 h to evaporate the liquid and dry the resulting residue.
7. After 48 h, reweigh the beaker with the residue. Remember: Don’t touch the beaker with bare hands.
8. Subtract the initial weight (in grams) of the empty beaker from the weight of the beaker with residue to obtain the increase in weight, or weight of the residue.
9. Convert the weight of the residue into mg/l using the following calculation
   Weight of residue x 1,000 mg x 1,000 mL = ? mg
   100 mL                       1 g               1 L             L

3. LabQuest Method for Measuring Turbidity

1. Turn on a LabQuest handheld monitor and plug-in the turbidity sensor into Channel 1, units should be NTU.
2. If units are not in NTU, use the stylus to touch the red area of the screen, select change units and choose NTU.
3. If units are in NTU, open the lid of the sensor and wipe-off (using a laboratory wipe) and insert the bottle that’s already filled with black printing on it (100 NTU), close lid.
4. Use the stylus to touch red area of screen and select Calibrate. When the calibration screen appears, select the Calibrate Now button (top left of the screen).
5. The cursor should have jumped to the first value box. Watch the voltage in the upper right corner of the screen. When it settles, use the stylus and the number keypad to type in 100. Then select the Keep button below.
6. The cursor should have jumped to the second value box. Now fill the second bottle with DI water (up to the line), cap-it, and wipe it off carefully using a laboratory wipe. Insert the DI water bottle into the sensor, and close the lid. When the voltage settles, type in 0 and press the Keep button.
7. Then press the OK button at the bottom right of the screen. Calibration is complete.
8. Discard the DI water from the second bottle and pour in just a splash of your water sample to rinse the bottle to rinse any remaining DI water and then discard sample rinse water. Then re-fill the bottle up tot the line with your water sample, re-cap, wipe-off (using laboratory wipes), and insert into the sensor. Close the lid and once the reading appears to settle, record the measurement.

4. LabQuest Method for Measuring Total Dissolved Solids Using Conductivity

1. For Total Dissolved Solids (TDS) using conductivity: Be sure the switch on the box (attached to your probe cord) is set to the bottom setting (0-2,000).
2. Plug the probe into channel 1. Units should be in milligrams per liter (mg/L).
3. If units are not in mg/L, use the stylus to touch the red area of the screen, select change units and choose mg/L.
4. If units are in mg/L, submerge the probe into your water sample and when the readings appear to stabilize record your measurement.