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Journal / Chemistry / Preparação de células líquidas de micropoços…
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Chemistry

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Preparação de células líquidas de micropoços suportadas por grafeno para microscopia eletrônica de transmissão in situ

Article DOI: 10.3791/59751-v • 08:30 min • July 15th, 2019
July 15th, 2019 •
*1, *1, 2, 3, 3, 1,2,4
1Electron Devices (LEB), Department of Electrical, Electronic and Communication Engineering, Friedrich-Alexander University Erlangen-Nürnberg, 2Fraunhofer Institute for Integrated Systems and Device Technology (IISB), 3Institute of Micro- and Nanostructure Research (IMN) and Center for Nanoanalysis and Electron Microscopy (CENEM), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg, 4Power Electronics (LEE), Department of Electrical, Electronic and Communication Engineering, Friedrich-Alexander University Erlangen-Nürnberg
* These authors contributed equally

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Um protocolo para a preparação de pilhas líquidas Graphene-suportadas do micropoço para a microscopia de elétron in situ de nanocristais do ouro da solução do precursor de haucl4 é apresentado. Além disso, uma rotina da análise é apresentada para quantificar a gravura observada e a dinâmica de crescimento.

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Química edição 149 célula líquida TEM in situ nanopartículas síntese condicionamento crescimento ouro cinética grafeno dendrite rastreamento de partículas únicas
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