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Journal / Biochemistry / Hydrolyseprodukter af en Ni-Schiff-Base Complex…
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Biochemistry

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JoVE Journal Biochemistry
Hydrolyseprodukter af en Ni-Schiff-Base Complex Brug af betingelser egnet til Bevarelse af syrelabile Protecting Groups
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Hydrolyseprodukter af en Ni-Schiff-Base Complex Brug af betingelser egnet til Bevarelse af syrelabile Protecting Groups

Article DOI: 10.3791/55677-v • 06:44 min • April 6th, 2017
April 6th, 2017 •
1, 1, 1
1Department of Chemistry, Slippery Rock University

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Her præsenteres en effektiv hydrolyse og efterfølgende Fmoc beskyttelse af en aminosyre isoleret fra en Ni-Schiff-basen kompleks. Hydrolysebetingelser præsenteret her, er egnede til anvendelse, når tilbageholdelse af syrelabilt sidekæde-beskyttende grupper er påkrævet. Denne teknik kan være tilpasses en række unaturlige aminosyre-substrater.

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Biokemi Schiff-base hydrolyse nikkel naturlig aminosyre syntese sidekædebeskyttende gruppe
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