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Forberedelse af stabile bicykliske Aziridinium ioner og deres Ring-åbning for syntese af Azaheterocycles
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Forberedelse af stabile bicykliske Aziridinium ioner og deres Ring-åbning for syntese af Azaheterocycles

Article DOI: 10.3791/57572-v • 11:45 min • August 22nd, 2018
August 22nd, 2018 •
1, 2
1Department of Chemistry, North Eastern Regional Institute of Science and Technology, 2Department of Chemistry, Hankuk University of Foreign Studies

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Bicykliske aziridinium ioner som 1-azoniabicyclo [4.1.0] heptan tosylate blev genereret fra 2-[4-tolenesulfonyloxybutyl] aziridine, som blev udnyttet til fremstilling af substituerede piperidines og azepanes via regio- og stereospecific ring-udvidelse med forskellige nukleofiler. Denne højeffektive protokol tillod os at forberede forskellige azaheterocycles herunder naturlige produkter som fagomine, febrifugine analog og balanol.

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Kemi spørgsmålet 138 bicykliske aziridinium ioner ring-ekspansion stereospecific azaheterocycles piperidines azepane
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