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In situ透過型電子顕微鏡を用いた全固体電池用コーティングのスクリーニング
JoVE Journal
Chemistry
This content is Free Access.
JoVE Journal Chemistry
Screening of Coatings for an All-Solid-State Battery Using In Situ Transmission Electron Microscopy
DOI:

07:20 min

January 20, 2023

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Chapters

  • 00:04Introduction
  • 01:00Preparation of Half‐Cut TEM Grids with Coated Si Nanoparticles for Checking the Suitability of ALD‐Deposited Titanium Dioxide Coatings
  • 01:53Preparing the Tungsten Needle
  • 02:37Loading the Drop‐Casted TEM Grid and Lithium Loaded Tungsten Needle into the In Situ TEM Holder
  • 03:15Inserting the Assembled In Situ Holder into the TEM
  • 04:02Performing the In Situ Biasing Experiment in the TEM and Analyzing the TEM Images
  • 05:37Results: Screening Method of Potential Coatings for All‐Solid‐State Batteries Using In Situ Transmission Electron Microscopy
  • 06:28Conclusion

Summary

Automatic Translation

本プロトコルは、(脱)リチウム化中のSiナノ粒子の体積変化を利用して、 in situ 透過型電子顕微鏡を用いた全固体電池の電位コーティングのスクリーニング方法を記載する。

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