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反应执行使用连续流处理的实时监控:3 - 乙酰基香豆素的制备为例
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JoVE Journal
Chemistry
Real-time Monitoring of Reactions Performed Using Continuous-flow Processing: The Preparation of 3-Acetylcoumarin as an Example
Please note that all translations are automatically generated.
Click here for the English version.
反应执行使用连续流处理的实时监控:3 - 乙酰基香豆素的制备为例
DOI:
10.3791/52393-v
•
09:56 min
•
November 18, 2015
•
Trevor A. Hamlin
,
Nicholas E. Leadbeater
1
Department of Chemistry
,
University of Connecticut
Chapters
00:05
Title
00:50
Find Suitable Signals for Reaction Monitoring and Interface the Raman Spectrometer with the Flow Cell
02:38
Prepare the Flow Apparatus
06:07
Monitor the Reaction and Data Analysis
07:50
Results: Real-time Monitoring of the Preparation of 3-Acetylcoumarin Using Continuous-flow Processing
09:16
Conclusion
Summary
Automatic Translation
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Automatic Translation
实时监控允许使用连续流动处理进行的反应的快速优化。这里的3-乙酰基香豆素,制剂被用作示例。用于进行
原位
拉曼监测装置进行说明,因为都是以优化反应所需的步骤。
Tags
Continuous-flow Processing
Inline Monitoring
Raman Spectrometry
3-acetylcoumarin Synthesis
Piperidine-catalyzed Reaction
Real-time Monitoring
Flow Unit
Flow Cell
Isothermal Conditions
Optimization
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