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Journal / Chemistry / Adgang Værdifuld ligand Understøtter for…
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JoVE Journal Chemistry
Adgang Værdifuld ligand Understøtter for Overgangsmetaller
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Adgang Værdifuld ligand Understøtter for Overgangsmetaller: En modificeret, Intermediate Scale Udarbejdelse af 1,2,3,4,5-Pentamethylcyclopentadiene

Article DOI: 10.3791/55366-v • 09:45 min • March 20th, 2017
March 20th, 2017 •
1, 1, 1
1Department of Science, Mount St. Mary's University

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Pålidelig, udarbejdelse af 1,2,3,4,5-pentamethylcyclopentadiene (Cp * H) mellemliggende skala præsenteres. Den reviderede protokol til syntese og oprensning af liganden minimerer behovet for specialiseret laboratorieudstyr samtidig forenkle reaktion workups og produkt rensning. Anvendelse af Cp * H ved syntesen af [Cp * MCL 2] 2 komplekser (M = Ru, Ir) er også beskrevet.

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Kemi Cp * H Iridium Ligand Pentamethylcyclopentadiene ruthenium Synthesis Overgangsmetaller
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