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DOI: 10.3791/60648-v
This article presents a detailed protocol for fabricating nano-height channels using surface acoustic wave actuation on lithium niobate for acoustic nanofluidics. The method includes room temperature plasma surface activated multilayer bonding, which is applicable for bonding lithium niobate to various oxides.
We demonstrate fabrication of nanoheight channels with the integration of surface acoustic wave actuation devices upon lithium niobate for acoustic nanofluidics via liftoff photolithography, nano-depth reactive ion etching, and room-temperature plasma surface-activated multilayer bonding of single-crystal lithium niobate, a process similarly useful for bonding lithium niobate to oxides.
Our protocol provides a detailed fabrication method of nano-height channels incorporating surface acoustic wave actuation via lithium niobate for acoustic nanofluidics. This technique can be used to perform room temperature plasma surface activated multilayer bonding of single crystal lithium niobate, a process equally useful for bonding lithium niobate or silicon dioxide and other oxides. Any debris and particulates should be removed during the cleaning and plasma surface activated processes to prevent bonding failure in the nano-height channel formation.
Visual demonstration of this method can capture the entire fabrication process in detail resulting in a clear presentation of the protocol for other researchers. To prepare a nano-height channel mask, place a wafer inscribed with a pattern designed to be a normal photolithography in liftoff procedures into a sputter deposition system and draw down the chamber vacuum to five times 10 to the negative six millitorr. Allow argon to flow at 2.5 millitorr and sputter chromium at 200 watts to produce a 400 nanometer thick sacrificial mask within 18 minutes.
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