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Chemistry

Préparation de nanoparticules de silice Grâce assistée par micro-ondes acide catalyse

Published: December 16, 2013 doi: 10.3791/51022
Automatic Translation
1, 2, 3, 3, 3
1Oak Ridge Institute for Science and Education, 2Air Force Research Laboratory, Airbase Technology Division, 3School of Materials Science and Engineering, Clemson University

Materials

Name Company Catalog Number Comments
Tetramethylorthosilicate Sigma Aldrich 218472
Hydrochloric acid, 37% Sigma Aldrich 435570
Acetone Fisher A949SK
Sulfuric acid EMD Millipore SX1244
Hydrogen peroxide, 30% EMD Millipore HX0635
Discover microwave reactor CEM
10 ml Borosilicate reaction vial CEM 908035
10 ml Snap cap CEM 909210
3 mm Stir bar Fisher Scientific 14-513-65
Highly polished silicon wafers Broker SP064483
S4800 SEM Hitachi
Zetasizer Nano90 Malvern
Polystyrene cuvette, (10 mm x 10 mm x 45mm) Sarstedt 67.754
5415D centrifuge Eppendorf
Hummer 6.2 sputter system Anatech

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References

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Préparation de nanoparticules de silice Grâce assistée par micro-ondes acide catalyse
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Cite this Article

Lovingood, D. D., Owens, J. R.,… More

Lovingood, D. D., Owens, J. R., Seeber, M., Kornev, K. G., Luzinov, I. Preparation of Silica Nanoparticles Through Microwave-assisted Acid-catalysis. J. Vis. Exp. (82), e51022, doi:10.3791/51022 (2013).

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