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Chemistry

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Synthesis and Characterization of Functionalized Metal-organic Frameworks
 

Synthesis and Characterization of Functionalized Metal-organic Frameworks

Article doi: 10.3791/52094
September 5th, 2014

Summary September 5th, 2014

Synthesis, activation, and characterization of intentionally designed metal-organic framework materials is challenging, especially when building blocks are incompatible or unwanted polymorphs are thermodynamically favored over desired forms. We describe how applications of solvent-assisted linker exchange, powder X-ray diffraction in capillaries and activation via supercritical CO2 drying, can address some of these challenges.

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