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Chapters
- 00:05Title
- 01:33Synthesis of Ynone
- 03:40Aqueous Workup
- 04:47Purification of Ynone
- 07:34Characterization of Ynone
- 08:17Results: Preparation of Ynones from Acyl Chlorides and Alkynyltrifluoroborate Salts
- 09:34Conclusion
The goal of this manuscript is to demonstrate a straightforward method for the preparation of ynones from acyl chloride and potassium alkynyltrifluoroborate salt starting materials. The one-pot reaction proceeds rapidly in the presence of boron trichloride without exclusion of air and moisture.
