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Forberedelse af DMMTAV og DMDTAV bruger DMAV for miljømæssige programmer
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Forberedelse af DMMTAV og DMDTAV bruger DMAV for miljømæssige programmer: syntese, rensning og bekræftelse

Article DOI: 10.3791/56603-v • 06:23 min • March 9th, 2018
March 9th, 2018 •
1, 2, 1, 1
1Korea Basic Science Institute, Seoul Center, 2Natural Science Research Institute, Yonsei University

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Denne artikel præsenterer modificerede eksperimentelle protokoller til dimethylmonothioarsinic syre (DMMTAV) og dimethyldithioarsinic syre (DMDTAV) syntese, inducerende dimethylarsinic syre (DMAV) thiolation gennem blanding af DMAV , Na2S og H2så4. Den ændrede protokol giver en eksperimentel retningslinje, derved at overvinde begrænsninger af trinene syntese, der kunne have forårsaget eksperimentelle fejl i kvantitativ analyse.

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Miljøvidenskab sag 133 Dimethylated thioarsenicals dimethylmonothioarsinic syre dimethyldithioarsinic syre syntese HPLC-ICP-MS ESI-MS
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