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Bioengineering
锰氧化物纳米粒子合成锰(II)乙酰酸盐的热分解
锰氧化物纳米粒子合成锰(II)乙酰酸盐的热分解
JoVE Journal
Bioengineering
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JoVE Journal Bioengineering
Manganese Oxide Nanoparticle Synthesis by Thermal Decomposition of Manganese(II) Acetylacetonate

锰氧化物纳米粒子合成锰(II)乙酰酸盐的热分解

Full Text
13,817 Views
09:02 min
June 18, 2020

DOI: 10.3791/61572-v

Celia Martinez de la Torre1, Margaret F. Bennewitz1

1Department of Chemical and Biomedical Engineering,West Virginia University

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Please note that some of the translations on this page are AI generated. Click here for the English version.

该协议详细说明了锰氧化物(MnO)纳米粒子的一个简单、单锅合成,在甲胺和二苯醚存在的情况下,对锰(II)乙酰乙酰酸盐进行热分解。MnO 纳米粒子已用于各种应用,包括磁共振成像、生物感应、催化、电池和废水处理。

与其他合成方法相比,热分解产生均匀的金属氧化物纳米颗粒,严格控制颗粒大小、形状和化学成分。这种技术是一个简单的锅合成,使用三种试剂,金属前体,有机溶剂和稳定剂。它可以产生不同类型的纳米颗粒,包括氧化锰和氧化铁。

展示这个程序的将是西莉亚·马丁内斯·德拉托雷,一个研究生研究助理在我的实验室。在开始实验之前,将四颈500毫升圆形底瓶放在加热地衣上。用金属爪夹固定中颈。

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