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Syntheses, Crystallization, and Spectroscopic Characterization of 3,5-Lutidine N-Oxide Dehydrate
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JoVE Journal Chemistry
Syntheses, Crystallization, and Spectroscopic Characterization of 3,5-Lutidine N-Oxide Dehydrate

Syntheses, Crystallization, and Spectroscopic Characterization of 3,5-Lutidine N-Oxide Dehydrate

DOI:
10.3791/57233-v

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06:18 min

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April 24, 2018

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, ,
1Centro de Química, Instituto de Ciencias,Benemérita Universidad Autónoma de Puebla

Chapters

  • 00:04Title
  • 01:14Reaction
  • 02:19Basicity Adjustment and Extraction
  • 03:17Crystallization Process and Analysis of 3,5-Lutidine N-oxide Dehydrate
  • 04:25Results: Characterization of 3,5-Lutidine N-Oxide Dehydrate
  • 05:51Conclusion

Summary

Automatic Translation

Automatic Translation

Herein, we report the synthesis and crystallization of 3,5-lutidine N-oxide dehydrate by a simple protocol that differs from the classical synthesis of pyridine N-oxide. This protocol utilizes different starting material and involves less reaction time to yield a new solvated supramolecular structure, which crystallizes under slow evaporation.

Tags

Keywords: 35-lutidine N-oxide DehydrateSolvated Supramolecular StructureSynthetic Organic ChemistryInorganic Chemistry2-aminopyridine-35-dicarboxylic AcidGlacial Acetic Acid35-dimethylpyridineHydrogen PeroxideHigh-vacuum DistillationSodium CarbonateChloroformSodium SulfateDiethyl EtherCrystallization

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