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配体介导成核与钯金属纳米粒子的生长
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Chemistry
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JoVE Journal
Chemistry
Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles
Please note that all translations are automatically generated.
Click here for the English version.
配体介导成核与钯金属纳米粒子的生长
DOI:
10.3791/57667-v
•
11:54 min
•
June 25, 2018
•
Saeed Mozaffari*
1
,
Wenhui Li*
1
,
Coogan Thompson
,
Sergei Ivanov
,
Soenke Seifert
,
Byeongdu Lee
,
Libor Kovarik
,
Ayman M. Karim
1
Department of Chemical Engineering
,
Virginia Polytechnic Institute and State University
,
2
Center for Integrated Nanotechnologies
,
Los Alamos National Laboratory
,
3
Advanced Photon Source
,
Argonne National Laboratory
,
4
X-ray Science Division
,
Argonne National Laboratory
,
5
Environmental Molecular Science Laboratory
,
Pacific Northwest National Laboratory
Chapters
00:04
Title
00:44
Palladium(II) Acetate Recrystallization
03:54
Colloidal Pd Nanoparticle Synthesis in Pyridine
06:25
Pd Nanoparticle Characterization by
Ex Situ
Small-Angle X-Ray Scattering (SAXS)
09:52
Results: Kinetics of Nucleation and Growth of Pd Nanoparticles in Toluene and Pyridine
11:20
Conclusion
Summary
Automatic Translation
English (Original)
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Automatic Translation
本研究的主要目的是通过结合 i.
原位
小角 x 射线散射 (SAXS) 和配体的动力学建模, 阐明封盖剂在调节钯纳米粒子尺寸中的作用。
Tags
Palladium
Nanoparticles
Nucleation
Growth
SAXS
Kinetic Rates
Capping Ligands
Colloidal
Metal Oxides
Palladium Acetate
Vacuum Filtration
Crystallization
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