A subscription to JoVE is required to view this content. Sign in or start your free trial.
1Department of Chemical Engineering,Virginia Polytechnic Institute and State University, 2Center for Integrated Nanotechnologies,Los Alamos National Laboratory, 3Advanced Photon Source,Argonne National Laboratory, 4X-ray Science Division,Argonne National Laboratory, 5Environmental Molecular Science Laboratory,Pacific Northwest National Laboratory
Chapters
- 00:04Title
- 00:44Palladium(II) Acetate Recrystallization
- 03:54Colloidal Pd Nanoparticle Synthesis in Pyridine
- 06:25Pd Nanoparticle Characterization by Ex Situ Small-Angle X-Ray Scattering (SAXS)
- 09:52Results: Kinetics of Nucleation and Growth of Pd Nanoparticles in Toluene and Pyridine
- 11:20Conclusion
Het belangrijkste doel van dit werk is het ophelderen van de rol van de aftopping van de agenten bij het reguleren van de grootte van palladium nanodeeltjes door het combineren van ikn situ kleine hoek x-ray scattering (SAXS) en ligand gebaseerde kinetische modellering.
