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High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy
JoVE Journal
Chemistry
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JoVE Journal Chemistry
High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy
DOI:

08:55 min

October 09, 2020

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Chapters

  • 00:04Introduction
  • 00:55Solid Sample Pretreatment
  • 01:57Solid Sample Loading
  • 02:52NMR Rotor Charging
  • 04:58Magic Angle Spinning (MAS) NMR Experiment
  • 05:46Results: Representative In Situ 1H and 13C MAS NMR Analyses
  • 07:49Conclusion

Summary

Automatic Translation

The molecular structures and dynamics of solids, liquids, gases, and mixtures are of critical interest to diverse scientific fields. High-temperature, high-pressure in situ MAS NMR enables detection of the chemical environment of constituents in mixed phase systems under tightly controlled chemical environments.

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