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用干冰作为固体 CO2源实现密封容器中的适度压力
JoVE Journal
Chemistry
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JoVE Journal Chemistry
Achieving Moderate Pressures in Sealed Vessels Using Dry Ice As a Solid CO2 Source
DOI:

06:26 min

August 17, 2018

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Chapters

  • 00:04Title
  • 00:50Reaction in a 7.5-mL Vial (Air Not Excluded)
  • 02:33Reaction in a 7.5-mL Vial (Purging Conditions – Air Excluded)
  • 03:34Reaction in a 35-mL Pressure Tube (Air Not Excluded)
  • 05:08Results: Representative 1H NMR Reaction Analyses
  • 05:46Conclusion

Summary

Automatic Translation

在这里, 我们提出了一个协议, 以执行反应的简单反应容器在低到中等压力的 CO2。这种反应可以通过在各种容器中进行, 只需以干冰的形式管理二氧化碳, 而不需要昂贵的或精密的设备或装置。

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