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Journal
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Chemistry
/
用干冰作为固体 CO
2
源实现密封容器中的适度压力
JoVE Journal
Chemistry
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JoVE Journal
Chemistry
Achieving Moderate Pressures in Sealed Vessels Using Dry Ice As a Solid CO
2
Source
Please note that all translations are automatically generated.
Click here for the English version.
用干冰作为固体 CO
2
源实现密封容器中的适度压力
DOI:
10.3791/58281-v
•
06:26 min
•
August 17, 2018
•
Mohit Kapoor
2
,
Pratibha Chand-Thakuri*
1,2
,
Justin M. Maxwell*
1,2
,
Michael C. Young
2
1
Department of Chemistry and Biochemistry
,
University of Toledo
,
2
School of Green Chemistry and Engineering
,
University of Toledo
Chapters
00:04
Title
00:50
Reaction in a 7.5-mL Vial (Air Not Excluded)
02:33
Reaction in a 7.5-mL Vial (Purging Conditions – Air Excluded)
03:34
Reaction in a 35-mL Pressure Tube (Air Not Excluded)
05:08
Results: Representative
1
H NMR Reaction Analyses
05:46
Conclusion
Summary
Automatic Translation
English (Original)
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Automatic Translation
在这里, 我们提出了一个协议, 以执行反应的简单反应容器在低到中等压力的 CO
2
。这种反应可以通过在各种容器中进行, 只需以干冰的形式管理二氧化碳, 而不需要昂贵的或精密的设备或装置。
Tags
Dry Ice
CO2 Atmosphere
Synthetic Organic Chemistry
Carbon Dioxide
Solid CO2 Source
Moderate Pressures
Sealed Vessels
CH Arylation
CH Capitulation
Epoxides
Syntha Carbonates
Palladium Acetate
Silver Trifluoroacetate
Phenyl Iodide
Tert-amylamine
Acetic Acid
Deionized Water
PTFE Cap
Room Temperature
Elevated Temperature
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